Albert Manero wins Fulbright Fellowship to conduct doctoral research at DLR in Cologne, Germany
Author Archives Seetha Raghavan
Our students present at MAE Research Day, win 1st and 2nd place awards
Congratulations to Sanna Siddiqui for winning 1st place for best research presentation, and congratulations to Alex Selimov for winning 2nd place for best poster.
The Department of Mechanical and Aerospace Engineering (MAE) hosts an annual research symposium. This is an opportunity for graduate and undergraduate researchers to present their work through a presentation or a research poster.
This year, a number of graduate and undergraduate students participated from our lab either with a presentation or a research poster. Sanna, Stephen, Imad, Alex, and Pascal were among those who presented at MAE research.
MAE Research Day 2015 @ UCF
The Department of Mechanical and Aerospace Engineering (MAE) presents Graduate and Undergraduate Research Day:
Morning Session: 9:00am-12:20pm
Poster Session: 12:20pm-2:00pm
Afternoon Session: 2:00pm-5:00pm
Imad wins UCF DURA
Congratulations to Imad Hanhan for being awarded the UCF Distinguished Undergraduate Research Award (DURA) for the month of February, 2015. Imad was chosen based on the overall merit of the research he is currently conducting as an undergraduate at UCF.
Students can apply for this award through the Office of Undergraduate Research (OUR), and are chosen from a panel of their peers.
DLR Guests Visit UCF
Collaborators and guests Dr.-Ing Marion Bartsch, Dr.-Ing Uwe Schulz, Dr.-Ing Stefan Hackemann, and Katia Artzt from DLR (German Aerospace Center) visited UCF, and presented a panel presentation on current trends in high temperature materials research.
Our collaborative work with DLR in combining synchrotron X-rays with a recreated engine environment was featured as the cover story in the January 2015 ACerS bulletin. Read our article in the ACerS Bulletin: Inside the engine environment – Synchrotrons reveal secrets of high-temperature ceramic coatings.
UCF graduate student Albert Manero is currently in Germany at DLR conducting research in high temperature materials with support awarded through the US Fulbright program.
ICACC 2015 @ Daytona
Scitech 2015 @ Orlando
Erik, Greg, and Stephen present at SciTech 2015
The Largest Event for Aerospace Research, Development, and Technology.
Check out our conference publications from SciTech 2015:
- Comparison of Thermal Barrier Coating Stresses via High Energy X-Rays and Piezospectroscopy.
Presented by Stephen Sofronsky - Damage Mapping of Composites with Piezospectroscopic Coatings.
Presented by Dr. Gregory Freihofer - Particle Size Effect on Load Transfer in Single Particle Composite Samples via X-Ray Diffraction.
Presented by Erik Durnberg
High School Student Mentored in Microwave Propulsion Physics
Jack – a Hagerty high school senior mentored by Imad – is currently investigating the underlying physical theories of microwave propulsion in order to produce a more efficient and more powerful propulsion device.
This research could potentially provide a more viable alternative method of satellite propulsion as well as develop our understanding of electrodynamics and the quantum vacuum.
ACerS Cover Story: Our High Temperature Materials Research
Our research on high temperature coatings is the cover story on Ceramic-tech Bulletin Jan/Feb 2015
Portable Piezospectroscopy system: non-contact in-situ stress sensing through high resolution photo-luminescent mapping
Read our paper in the Journal of Instrumentation
Through the piezospectroscopic effect, certain photo-luminescent materials, once excited with a laser, produce spectral emissions which are sensitive to the stress or strain that the material experiences. A system that utilizes the piezospectroscopic effect for non-contact stress detection over a material’s surface can capture important information on the evolution of mechanical response under various conditions. Therefore, the components necessary for piezospectroscopic mapping and analysis have now been integrated into a versatile and transportable system that can be used with photo-luminescent materials in any load frame or on a variety of structures. This system combines compact hardware components such as a portable laser source, fiber optics, spectrograph, charge-coupled device (CCD), and an X-Y-Z stage (with focusing capabilities) with a series of data analysis algorithms capable of analyzing and outputting high resolution photo-luminescent (PL) maps on-site. Through a proof of concept experiment using a compressed polycrystalline alumina sample with sharp machined corners, this system successfully captured high resolution PL maps with a step size of 28.86 μm/pixel and located high stress concentrations in critical areas, which correlated closely with the results of a finite element model. This work represents an important step in advancing the portability of piezospectroscopy for in-situ and non-contact stress detection. The instrumentation developed here has strong implications for the future of non-destructive evaluation and non-invasive structural health monitoring.
Alex Selimov, funded by the ICubed program, works with art students to create prints based on the lab’s work
Alex Selimov presented to and worked with students from Professor Dennis Ahearn’s Advanced Printmaking class in order to create prints based on Piezospectroscopy and Thermal Barrier Coatings. This work was funded by ICubed and will be presented at a showcase during the Spring. ICubed is a NSF funded project whose project goal is to ensure broader impact of NSF funded projects through coordination and integration of the education and research activities of these funded projects by increasing participation in Science, Technology, Engineering and Mathematics (STEM) fields.
Research students volunteered to instruct Solid Mechanics labs
Students conducting research volunteered to teach students taking the lab for solid mechanics about Piezospectroscopy. 3 groups of students were taught over two weeks. They learned about how Piezospectroscopy can be used for both tension and compression. The students who instructed the labs were Imad Hanhan, Alex Bullock, Sanna Siddiqui, Stephen Sofronsky, Pascal Fouquet, Alex Selimov, and Mateo Alvarez.
Gregory Freihofer, recently graduated with a PhD in Mechanical engineering wins 2nd place award at SAMPE CAMX student competition
Gregory Freihofer wins 2nd place at the SAMPE CAMX student paper competition
Gregory Freihofer, recently graduated with a PhD in Mechanical engineering wins 2nd place award at SAMPE CAMX student competition.
Gregory Freihofer, a recent PhD graduate from the Aerostructures lab, wins second place at the SAMPE CAMX conference in the student research symposium. CAMX stands for The Composites and Advanced Materials Expo and is a conference that is dedicated for the advancement of all aspects of composites and advanced materials. The student research symposium is a competitive program that sponsors students to present the results of their technical research. Gregory won a cash prize of $1,000 for his work.
Stephen and Greg Spend Summer at Boeing Seattle as part of NSF GOALI Research
Stephen and Greg Spend Summer at Boeing Seattle as part of NSF GOALI Research
Stephen and Greg Spend Summer at Boeing Seattle as part of NSF GOALI Research
Stephen traveled to Seattle to conduct experiments at the shock physics lab in Boeing Seattle with Gregory Freihofer and the shock physics team: Dr. Housen Bill Sweet, Dr. Damazo and Wayne Campbell, These experiments take the NSF funded GOALI Research on “Developing piezospectroscopic adhesives and coatings” and tests it in the dynamic region. The high strain rates experiments were conducted with the shock physics lab’s split Hopkinson bar and the lab’s portable spectrometer.
Novel capability enables first test of real turbine engine conditions – Featured on Office of Science Homepage
The Office of Science , Department of Energy has featured our work on their homepage.
The article highlights our work:
“This goes beyond any other in-situ capabilities to allow the influence of temperature, stress and thermal gradients to be studied together. This enables for the first time scientists to view the microstructure and internal strain in both the substrate and thermal barrier coating system during real operating conditions and in real time.”
Read more of the article on the ANL webpage
Students Mentored through LEARN program
Through the Learning Environment and Academic Research Network (LEARN) program, Imad is mentoring two first year students. The two students, Steven and Luke, are working on a research project regarding the photoluminescent characterization of a hybrid carbon fiber composite, as well as developing graphical user interfaces for non-linear least squared software analysis
Multiscale mechanics to determine nanocomposite elastic properties with piezospectroscopy
Read our paper in Acta Materialia
Abstract:
The piezospectroscopic (PS) properties of chromium-doped alumina allow for embedded inclusion mechanics to be revisited with unique experimental setups that probe the particles’ state of stress when the composite is under applied load. These experimental investigations of particle mechanics will be compared to the Eshelby theory and a derivative theory. This work discovers that simple nanoparticle load transfer theories are adequate for predicting PS properties in the low to intermediate volume fraction range (⩽20%). By applying the multiscale mechanics to a PS response, the inverse problem was demonstrated to reveal the elastic modulus of the composite. The implications for this technique are damage monitoring through observation of reduced mechanical properties in addition to a method to assist with engineering nanomaterials.
Our work featured in ACerS Ceramic Tech Today
Our international collaboration and recent paper in Nature Communications has been featured in ACerS Ceramic tech today.
Read the full article here.
Capturing High Temperature Coating Strains under Extreme Engine Environments
Read our Nature Communications article
UCF today highlights our work.
Our work and international collaboration was featured on the Ceramic-tech-today
Abstract
The mechanical behaviour of thermal barrier coatings in operation holds the key to understanding durability of jet engine turbine blades. Here we report the results from experiments that monitor strains in the layers of a coating subjected to thermal gradients and mechanical loads representing extreme engine environments. Hollow cylindrical specimens, with electron beam physical vapour deposited coatings, were tested with internal cooling and external heating under various controlled conditions. High-energy synchrotron X-ray measurements captured the in situstrain response through the depth of each layer, revealing the link between these conditions and the evolution of local strains. Results of this study demonstrate that variations in these conditions create corresponding trends in depth-resolved strains with the largest effects displayed at or near the interface with the bond coat. With larger temperature drops across the coating, significant strain gradients are seen, which can contribute to failure modes occurring within the layer adjacent to the interface.
Imad’s SURF experience @ Purdue
This summer Imad traveled to Purdue University to participate in the Summer Undergraduate Research Fellowship (SURF) program. During this time, Imad worked in an aerospace laboratory under the direction of Dr. Michael Sangid in a project regarding Long Carbon Fiber Thermoplastic composites.
In August, Imad presented at the Purdue SURF symposium, and was awarded “Top Research Talk” (one of 5 awards out of 143 students).
Boeing Research
Ashley and Greg performed summer research at Boeing Seattle
Fulbright Fellowship
Albert Manero wins Fulbright Fellowship to conduct doctoral research at DLR in Cologne, Germany
International Collaboration – German Aerospace Center DLR
Sanna Siddiqui Presents at the 25th AeroMat Conference and Exposition
Sanna presented her research work on the “Impact of CMAS ingression on strain tolerance within the layers of a plasma sprayed Thermal Barrier Coating” at the 25th AeroMat Conference and Exposition held in June. The AeroMat conference showcased the latest developments in aerospace and materials processing.
Our posters at SURE 2014
This year at the Showcase of Undergraduate Research Excellence, our undergraduate researchers represented the lab with some amazing posters and presentation skills. SURE is a university wide poster presentation forum held annually at the University of Central Florida. The SURE event gives undergraduate students the opportunity to present the research they are working on and gives students a chance to learn more about the other research being conducted throughout the university. Pascal and Frank took home the honorable mention award this year.
Clockwise from top: Pascal and Frank, Imad, Alex Selimov and Alex Bullock, Michael and Drew and Jordan.
Showcase of Undergraduate Research Excellence (SURE 2014)
Pascal Fouquet presenting research on synchrotron analysis of thermal barrier coatings at the 2014 Showcase of Undergraduate Research Excellence (SURE) at UCF.
The presentation won honorable mention.
Albert Manero wins US Fulbright Fellowship to conduct research in Germany
Doctoral engineering student in the Mechanical and Aerospace Engineering Department at the University of Central Florida has been given the opportunity of a lifetime. Albert Manero has been offered the Fulbright Academic Grant Fellowship to Germany, where he will be working with the German Aerospace Center (DLR) as a part of his doctoral research in high temperature coatings for thermal protection systems with an application in jet turbine engines and for space planes. Albert has participated in an international collaboration with the German Aerospace Center since the summer of 2012 as part of our National Science Foundation OISE Catalyzing new international collaborations grant. His participation in the summer research experience in Cologne Germany set the foundation for a successful research relationship with joint publication outcomes. The Fulbright fellowship will provide Albert the opportunity to continue to forge this collaboration for his doctoral research.
Sanna, Kevin and Albert attend ICACC 2014
The 38th International conference and Expo on Advanced Ceramics and Composites was held January 27th at Daytona Beach. Organized by the American Ceramic Society’s Engineering Ceramics Division and ACerS, ICACC’14 showcased cutting-edge research and product developments in advanced ceramics, armor ceramics, solid oxide fuel cells, ceramic coatings, bioceramics and more. The topical areas include advanced structural and functional ceramics, composites and other emerging ceramic materials and technologies.. Kevin and Albert presented their research on “High Energy X-rays Characterizing the Material Behavior of High Temperature Thermal Barrier Coatings” and “Piezospectroscopy Measurement of Thermal Barrier Coating Systems.” Sanna, Kevin and Albert also had the opportunity to meet with our DLR collaborators.
Piezospectroscopic Measurements Capturing the Evolution of Plasma Spray-Coating Stresses with Substrate Loads
Our paper in Applied Materials & Interfaces highlights the evolution of stress within APS coatings under increasing substrate loads captured using piezospectroscopy.
Abstract
Plasma-spray coatings have a unique microstructure composed of various types of microcracks and weakly bonded interfaces which dictate their nonlinear mechanical properties. The intrinsic photo-luminescence (PL) characteristics of alpha-alumina (α-Al2O3) within these coatings offer a diagnostic functionality, enabling these properties to be probed experimentally at the microscale, under substrate loading. The piezospectroscopic (PS) measurements from the coatings are capable of revealing microstructural stress at high spatial resolution. Here, for the first time, the evolution of stresses within air plasma spray (APS) coatings under increasing substrate loads were captured using piezospectroscopy. With mechanical cycling of the substrate, the PS properties revealed anelastic and inelastic behavior and a relaxation of residual tensile stress within the APS coatings. With decreasing substrate thickness, the coating was observed to sustain more stress, as the substrate’s influence on the mechanical behavior decreased. The findings provide an insight into the microstructural response that can serve as the basis for model validation and subsequently drive the design process for these coatings.
Kevin, Greg and Erik Present at AIAA SCI-TECH 2014
AIAA SciTech 2014 was one of the largest events for Aerospace research, development, and technology. It included multiple keynotes by industry professionals from all around the nation and paper presentations showcasing research from 45 countries around the world. Erik presented a paper on low strain rate ALOX experiments which was a result of our labs collaboration with Eglin Air Force Base. Greg presented a paper on the work our lab has done with Boeing on carbon fiber open-hole tension samples and Kevin presented a paper on synchrotron TBC data gathered at Argonne National Laboratory with a collaboration with DLR (German Aerospace Center).
LEARN Students Obtain Hands On Experience
The LEARN Program at the University of Central Florida introduces freshmen students to STEM (Science, Technology, Engineering, & Mathematics) research and provides a hands on experience to challenge and prepare incoming students for both their academic and professional careers. Jennifer Santana and Jorge Torres [pictured on right] have been in the LEARN Program since the Fall of 2013, where they have learned the fundamentals of spectroscopy and its application for non-destructive testing in Dr. Seetha Raghavan’s Laboratory. Their Graduate Mentor, Albert Manero, has been quite excited by the progress they have made in such a short amount of time .
Our collaborative research featured in DLR’s magazine
Our research collaboration with DLR (German Aerospace Center), CSU and Argonne National Laboratory was featured in DLR’s latest magazine on their website. The NSF funded international collaboration that started with a summer research experience for the UCF team in Germany has successfully initiated in situ synchrotron measurements of thermal barrier coatings under thermal gradients an mechanical loads. The first of our publications in Review of Scientific Instruments is now available.Ongoing research will capture the strain evolution within the layers of these high temperature coating systems that protect turbine blades under jet engine operational conditions
Synchrotron X-ray measurement techniques for cylindrical samples under thermal gradients
This study displays the ability to monitor in situ, the response of the internal layers within a layered coating, while implementing a thermal gradient across the thickness of the coated sample. The thermal setup maintained coating surface temperatures in the range of operating conditions, while monitoring the substrate cooling, for a controlled thermal gradient. Read our paper here.
Abstract
Measurement techniques to obtain accurate in situ synchrotron strain measurements of thermal barrier coating systems (TBCs) applied to hollow cylindrical specimens are presented in this work. The Electron Beam Physical Vapor Deposition coated specimens with internal cooling were designed to achieve realistic temperature gradients over the TBC coated material such as that occurring in the turbine blades of aeroengines. Effects of the circular cross section on the x-ray diffraction (XRD) measurements in the various layers, including the thermally grown oxide, are investigated using high-energy synchrotron x-rays. Multiple approaches for beam penetration including collection, tangential, and normal to the layers, along with variations in collection parameters are compared for their ability to attain high-resolution XRD data from the internal layers. This study displays the ability to monitor in situ, the response of the internal layers within the TBC, while implementing a thermal gradient across the thickness of the coated sample. The thermal setup maintained coating surface temperatures in the range of operating conditions, while monitoring the substrate cooling, for a controlled thermal gradient. Through variation inmeasurement location and beam parameters, sufficient intensities are obtained from the internal layers which can be used for depth resolved strain measurements. Results are used to establish the various techniques for obtaining XRD measurements through multi-layered coating systems and their outcomes will pave the way towards goals in achieving realistic in situ testing of these coatings.
Ashley and Greg spend summer at Boeing Seattle as part of NSF GOALI Research
Ashley and Greg spent this summer conducting experiments for our research at the Applied Physics Laboratories in Boeing Seattle with the guidance of our collaborator Ms Hong Tat. These experiments are part of our ongoing NSF funded GOALI Research on “Developing piezospectroscopic adhesives and coatings”. The team brought with them our UCF-designed and integrated portable spectrometer system to collect piezospectroscopic measurements on samples under mechanical loads. This summer, faculty mentors Dr Raghavan and Dr Schülzgen took the opportunity to visit the site and meet with Boeing researchers. The results of their successful experiments will be presented at upcoming conferences.
Our Research presented at the Undergraduate Summer Research Academy
Sanna, Claudine, Matt, Forrest and Erik present the TBC and Alumina sensing coatings research at the Undergraduate Summer Research Academy Forum held at UCF. Albert and Frank presented an overview of the laboratory to undergraduate students touring the laboratory.
Visiting undergraduate researchers from Cleveland State University
Matt Smith and Claudine, Chemical Engineering majors from Cleveland State University (CSU) in Ohio are visiting undergraduate researchers in our laboratory this summer. As part of an ongoing collaboration among UCF, DLR Aerospace and CSU funded by the National Science Foundation’s OISE on Thermal Barrier Coatings research. Claudine graduated among the top percentile from St Croix Educational Complex High School in the US Virgin Islands. She is a recipient of the President’s List and Dean’s List honors from Cleveland State University. Matt is a member of AlChE and is currently working on the Cleveland State team for the AlChE Chemical Car competition. In his spare time he enjoys playing the guitar and video games as well as looking at the mathematical aspects of daily life.
Ashley and Greg present at SAMPE 2013, Long Beach, CA.
Our group presented two papers at the 2013 Society for the Advancement in materials and process engineering (SAMPE) conference in Long Beach, CA. “Prediction of Piezospectroscopic properties with nanoparticle load transfer theories” reports on some of the outcomes of our NSF GOALI research with Boeing Research and Technology and was presented by Greg. Ashley presented her original work on “Low Strain Rate in situ piezospectroscopic studies of Alumina Nanocomposites”
Kevin presents at 54th AIAA Structures and Structural Dynamics Conference 2013
The AIAA Structures, Structural Dynamics, and Materials Conference (SDM) provides a unique forum dedicated to the latest developments in the collective disciplines of structures, structural dynamics, materials, design engineering, and survivability. Kevin represented our research group at this event which was held in Boston with a presentation on “Simulations Mapping Stress Evolution in High Temperature Ceramic Coatings under Thermal-Mechanical Conditions”
MAE Research Day features 4 presentations and 1 poster from our group
This year’s Mechanical and Aerospace Engineering research day was held at the Live Oak Event Center and featured graduate student presentations from over 30 students. Albert served as one of the lead graduate co-ordinators of the event. Sanna, Kevin, Greg and Ashley presented their research at the forum. The lunchtime poster session had several graduate and undergraduate participants. Erik and Forrest presented their poster at this event.
Drew Thomas wins award for his poster presentation as part of the UCF LEARN program
Drew Thomas spent the last 2 semesters in our laboratory during his freshman year learning about research. This week marked the end of the LEARN program for Drew. The LEARN program at UCF is an initiative to encourage undergraduate freshmen to engage in research early within their area of discipline. Drew’s presentation was the award winner for the program and he was acknowledged for his demonstration of a great command of a challenging subject. His success is shared by his graduate mentors in our laboratory Sanna Siddiqui and Albert Manero who have nothing but praise for his efforts and enthusiasm. Drew’s words to his mentors: “Thanks for the great experience that I had over the course of the year and thank you for introducing me into the world of research.”
Erik, Forrest and Tim win 1st Place in UCF Showcase of Undergraduate Research in Engineering for Best Poster.
Erik Durnberg, along with co-presenters Forrest Vaughn and Timothy Johnson, received first place distinction in the College of Engineering and Computer Science Category at the Showcase of Undergraduate Research for their poster “Piezospectroscopy for Comparing Analytical and Numerical Nanoparticle Load Transfer Theories.”
The Showcase of Undergraduate Research Excellence is a university wide poster presentation held annually at the University of Central Florida. The SURE event gives undergraduate students the opportunity to present the research they are working on and gives students a chance to learn more about the other research being conducted throughout the university. This is the second year in a row that undergraduate students from our lab have won first place at the event.
Sanna Siddiqui wins prestigious 2013 National Science Foundation Graduate Research Fellowship
Sanna F. Siddiqui was recently awarded the prestigious National Science Foundation (NSF) Graduate Research Fellowship.
The NSF GRFP provides support for the graduate education of individuals who have demonstrated their potential for significant achievements in science and engineering research. The ranks of NSF Fellows include individuals who have made transformative breakthroughs in science and engineering research and have become leaders in their chosen careers and Nobel laureates
Sanna and Kevin present at ICACC 2013 in Daytona
The 37th International conference and Expo on Advanced Ceramics and Composites was held January 27th at Daytona Beach. Organized by the American Ceramic Society’s Engineering Ceramics Division and ACerS, ICACC’13 showcases cutting-edge research and product developments in advanced ceramics, armor ceramics, solid oxide fuel cells, ceramic coatings, bioceramics and more. The topical areas include advanced structural and functional ceramics, composites and other emerging ceramic materials and technologies..Sanna and Kevin present their research on the “Effect of Calcium-Magnesium-Alumina-Silicate on Strain within the TGO Layer of Thermal Barrier Coatings” and “Acquisition Techniques for Synchrotron X-ray Strain Measurements in Tubular TBC Specimens for Thermal Gradient Mechanical Testing”.
Dr Jennifer Jordan and Dr George Sunny from Eglin AFB, present a seminar at UCF
Along with Dr Gordon’s group at UCF, our group had the pleasure of hosting a visit from the Energetic Materials Branch within the Munitions Directorate, Air Force Research Laboratory at Eglin AFB. Dr Jennifer Jordan, internationally recognized for her research in high strain rate response of polymers and composites, presented a seminar on the “Mechanics of Particulate Composites”. Dr Sunny is responsible for the Mechanical testing laboratory for energetic materials and assists with the strategic direction for theoretical and computational efforts related to energetics at Eglin AFB. He presented a talk on “A High Strain-rate investigation of a Bulk Metallic Glass.”
UCF LEARN students active in TBC Research
The LEARN program at UCF is an initiative to encourage undergraduate freshman students to engage in research early within their area of discipline. Anselmo Crespin and Drew Thomas who are both freshman aerospace engineering students spent this semester learning about thermal barrier coatings and the process of data analysis as part of the LEARN program from their mentors Sanna Siddiqui and Albert Manero.
Albert and Kevin conduct pioneering in situ synchrotron thermal gradient mechanical experiments with DLR Aerospace and Argonne National Laboratory.
Albert and Kevin conduct pioneering in situ synchrotron thermal gradient mechanical experiments on thermal barrier coated specimens with our collaborators from DLR Aerospace (Germany) and Argonne National Laboratory.
Our NSF funded international collaboration with DLR (German Aerospace Center) and Argonne National Laboratory that started with a summer research experience for the UCF team in Germany comes full circle with the successful initiation of in situ synchrotron measurements at Argonne National Laboratory, Illinois. The first of a set of in situ experiments conducted under thermal gradients and mechanical loads at the 1-ID beamline of the Advanced Photon Source, the tests will capture the strain evolution within the layers of these high temperature coating systems that protect turbine blades under jet engine operational conditions.
Greg Freihofer spends summer at Boeing Research & Technology in Seattle as part of NSF GOALI research
This summer, Greg .and Amy gained research experience in Seattle under the guidance of our collaborator Hong Tat of the Applied Physics Non Destructive Evaluation group, Boeing Research & Technology as part of an NSF funded GOALI research project. In efforts to understand the applied research potential of the fundamental studies they have been conducting at UCF on stress sensing coatings, they were introduced to various techniques and standards used by the aerospace industry. Following their summer experience, they will continue their work on developing these coatings to monitor integrity of aerospace structures
Albert and Kevin spend summer at DLR Aerospace in Cologne, Germany
As part of a Catalyzing New International Collaborations award from NSF, Albert and Kevin spent their summer expanding their research knowledge in the area of high temperature coatings at DLR Aerospace, German Aerospace Center, Germany’s national research center for aeronautics and space research. Under the guidance of Dr Marion Bartsch, the students were provided opportunities to learn about coating processes, simulation and thermal gradient fatigue testing conducted at the advanced facilities. Their scientific experience was complemented with activities such as the DLR Annual company picnic and visits to Forschungszentrum Jülich and Siemens giving them an insight to the society, culture and language. The collaboration will lead to new techniques for in situ synchrotron measurements under thermal gradients and mechanical loads with collaborators at Argonne National Laboratory.
Our paper awarded 3rd place for 2012 Outstanding paper award at the SAMPE conference, Baltimore
Gregory Freihofer was given the opportunity to present two papers at the Society for the Advancement in materials and process engineering (SAMPE) conference in Baltimore this 2012. One of the papers that Greg presented “Embedded alumina nanoparticles as diagnostic coatings for structures” was awarded 3rd place for the Outstanding paper award at the SAMPE conference. Greg was able to proudly accept this award on behalf of his student co-authors Ashley Jones, Emrecan Ergin, Kevin Lautenslager, and Will Gysi and our collaborators Dr Schülzgen (CREOL) and Hong Tat (Boeing Reseearch & Technology).
Will Gysi and Steve Scott present their posters at the ANL User’s Conference
Steven Scott and Will Gysi attended the Argonne National Laboratory (ANL) User Meeting. World renown researchers and scientists were in attendance presenting their novel research. Both Steven and Will participated in workshops pertaining to the Advanced Photon Source and the Center for Nanoscale Materials. Steven presented his poster on “The Role of Thermo-mechanical Loads on Depth-resolved EB-PVD TBC’s – in situ Synchrotron Experiments” and Will presented his poster on “Stress-Sensing Nanomaterials using Photo-simulated Luminescence Spectroscopy.” The trip was an overall success and the experience and knowledge gained will be brought back to the UCF lab.
Our research video wins 1st place for best documentary in the “Usies” video competition at ANL’s Users Conference.
An outreach video made by our researchers “An Undergraduate Story” won Best Documentary in the ANL Users Meeting “Usies” Video Competition. The effort, led by Steven Scott, showcases undergraduate participation at Argonne National Laboratory made possible through our NSF funded research on high temperature coatings.It highlights the success of our undergraduate researchers and the opportunities for high impact research available to undergraduates. The video is showcased in our website video page.
Will, Kevin, Spencer and Erik win awards at the 2012 Showcase of Undergraduate Research Excellence
Will Gysi and Kevin Lautenslager received first place distinction at the Showcase of Undergraduate Research Excellence for their poster on “Stress-sensing Nanomaterials Using Photo-Stimulated Luminescence Spectroscopy” in the College of Engineering and Computer Science Category 1. Spencer Frank and Erik Durnberg received honorable mention for their poster on “A Theoretical Model of Load-Transfer in an Alumina Nanoparticle Filled Epoxy Matrix to Obtain Stress-Sensing Characteristics”.
The Showcase of Undergraduate Research Excellence is a poster presentation of undergraduate research held annually at the University of Central Florida. This showcase gives undergraduate students the opportunity to present the research they are currently working on.
Spencer Frank awarded 2012 National Science Foundation Graduate Research Fellowship
Spencer Frank been awarded the NSF Graduate research fellowship. The award will support Spencer as he pursues his PhD in Mechanical Engineering at UC Berkeley. With over 3 years of undergraduate research background in our laboratory with various contributions in areas of turbine blade flutter, piezospectroscopy and mechanics of nanocomposites, we know that Spencer is more than ready for his next endeavor. The program recognizes and supports outstanding students who are pursuing research-based master’s and doctoral degrees in fields within NSF’s mission. The GRFP provides support for the graduate education of individuals who have demonstrated their potential for significant achievements in science and engineering research. The ranks of NSF Fellows include individuals who have made transformative breakthroughs in science and engineering research and have become leaders in their chosen careers and Nobel laureates.
Talia Field presents at the AIAA SDM Conference in Honolulu, Hawaii
53rd AIAA/ASME/ASME/AHS/ASC Structures, Structural Dynamics, and Materials Conference: Materials Conference: This established annual conference is a widely acknowledged event that provides a unique forum dedicated to the latest developments in the collective disciplines of structures, structural dynamics, materials, design engineering, and survivability. Plenary presentations by recognized, forward-thinking invited speakers are a special feature of the conference. This year’s presentations were organized around the potential applications of structures, structural dynamics, and materials in the next generation of aircraft. Talia presented “Synchrotron X-rays Monitoring Nano-Aluminim Grain Growth of a Metal Matrix Composite under Thermo-mechanical conditions on behalf of her student co-authors, Ashley Jones and Melan Jansz.
Role of Mechanical Loads in inducing in-cycle tensile stress in thermally grown oxide
Abstract
Experimental in situ synchrotron x-ray diffraction results tracking the strain behavior of the various layers during a cycle, under thermo-mechanical conditions are presented in this work. The quantitative strain measurements here show that the thermally grown oxide briefly experiences in-plane tensile stress with increased mechanical loading during ramp-up in the thermal cycle. These findings are the first in situ experimental observations of these strains under thermo-mechanical conditions, envisaged to serve as a catalyst for crack initiation. The depth resolved measurements of strain taken during applied thermal and mechanical load in this work are a significant step towards achieving realistic testing conditions.
Read our paper in Applied Physics Letters
Will and Greg perform experiments at the Center of Nanoscale Materials, Argonne National Laboratory (CNM)
The trip to CNM was part of a collaboration with CNM scientists to develop nanoscale experiments to investigate the fundamentals of the stress sensing behavior for varying alumina nanoparticles. Using electron beam (E-beam) lithography, “nanobuckets” were created in Si wafers of various sizes and filled with an epoxy/alumina nanoparticle mixture.
The sample development will pave the way for experiments using an Atomic Force Microscope (AFM) within a confocal backscattering setup for measuring Photo-luminescence from the samples. These fundamental studies will investigate a range of particles, quantifying a multitude of important nano-composite properties such as interface strength, load transfer, and piezospectroscopic properties
Our paper selected as feature article in Polymer Journal
Our publication on the “Characterization of particle dispersion and volume fraction in alumina filled epoxy nanocomposites using photostimulated luminescence spectroscopy” was selected as a feature article by Polymer Journal.
The paper authored by Amanda Stevenson, Ashley Jones and S. Raghavan presents a novel method of evaluating the dispersion o alumina nanoparticles within a polymer matrix as well as creating a calibration for filler particle volume fraction. Polymer Journal publishes a wide variety of article types on cutting-edge developments in macromolecule research.
Fall Seminar – Dr. Anette Karlsson, Chair and Professor at the Department of Mechanical Engineering at the University of Delaware, visits UCF
As part of the MMAE Fall Seminar Series, Dr. Anette Karlsson visits UCF to present a lecture on “The microstructures of arthropod exoskeletons and the mechanical behavior of bio-inspired composites”. Dr. Karlsson visits the team’s lab to get an update on our work on Synchrotron XRD in-situ strain measurements of EB-PVD Thermal Barrier Coatings and on Characterization of alumina-filled epoxy nanocomposites using photo-stimulated luminescence spectroscopy.
International student joins research team
John Ergin is a graduate student from Chalmers University in Sweden, working in our lab as part of the ALOX team researching stress sensing coatings using photo-stimulated luminescence spectroscopy. John received his Bachelor’s Degree in Materials and Metallurgical Engineering at Yildiz Technical University in Turkey and is set to earn his Masters Degree in Advanced Engineering Materials at Chalmers University in June 2012. Welcome, John!
Characterization of particle dispersion and volume fraction in alumina-filled epoxy nano composites using photo-stimulated luminescence spectroscopy
Abstract
A novel method is presented to validate the dispersion of a-alumina nanoparticles within a polymer matrix, as well as to create a calibration for filler particle volume fraction identification. Using photo-stimulated luminescence spectroscopy (PSLS), spectral information from a-alumina-filled epoxy nanocomposites consisting of varying volume fraction quantities of alumina nanoparticles was collected and analyzed. Surface contour maps of each nanocomposite were created by comparing integrated intensity data from the R1 curve of a-alumina throughout each specimen. These maps show satisfactory dispersion of alumina in the 5 and 25% volume fraction composites, whereas agglomerations were detected in various regions of the 38% nanocomposite, establishing the capability of this method to characterize photo-luminescent particle dispersion. This new approach also provides high spatial resolution, which can be used to determine the exact locations of voids, inclusions and/or agglomerations, while also predicting the volume percentage of photo-luminescent particle content within a specimen, lending itself as a quality control method in the manufacturing of these composites.
Read the full paper at http://www.nature.com/pj/journal/v43/n11/full/pj201182a.html
Rene Diaz is UCF’s undergraduate researcher of the month for August 2011
Rene Diaz (recently graduated) has been nominated and chosen for the undergraduate of the month award based on the overall merit of the research he has conducted at UCF, entitled, “In-Situ Strain Measurements of EB-PVD Thermal Barrier Coatings using Synchrotron X-Ray Diffraction under Thermo-Mechanical Loading”. This award recognizes excellence in undergraduate research at the University of Central Florida and honors students who have excelled in academic research under the mentorship of a UCF faculty mentor. Rene will receive a certificate as well as a write-up in the Office of Undergraduate Research’s monthly newsletter and recognition on their website.
Stress-sensing nanomaterial
Read our paper in Nanoletters
Abstract
Calibration of high spatial resolution stress-sensing alumina-epoxy nanomaterials is presented. The piezospectroscopic property of luminescent chromium-doped alumina nanoparticles embedded as “nano-sensors” in epoxy-based materials is the basis for the stress sensing capabilities. The stress-optical properties are determined as piezopectroscopic coefficients in compression experiments for nanomaterials containing varying volume fractions of alumina nanoparticles. An increasing stress-sensitivity was demonstrated with higher volume fractions. Thermal variations were shown to have negligible effects on the stress sensing property. The development of this material sensing system will enable quantitative measurement and non-invasive monitoring of stress distributions within a polymer system applied as adhesives or as coatings on a substrate under loading conditions.
Ashley and Rene awarded prestigious 2011 NSF Graduate Research Fellowships
Ashley and Rene have been awarded NSF Graduate research fellowships. The program recognizes and supports outstanding students who are pursuing research-based master’s and doctoral degrees in fields within NSF’s mission. The GRFP provides support for the graduate education of individuals who have demonstrated their potential for significant achievements in science and engineering research. The ranks of NSF Fellows include individuals who have made transformative breakthroughs in science and engineering research and have become leaders in their chosen careers and Nobel laureates
Both Ashley and Rene are active undergraduate researchers working on high impact research in our laboratory. In addition to their excellent academic and research portfolio, they have been active in mentoring and volunteering efforts. Ashley’s research has been funded by the UCF Office of Research and Commercialization In-house Research Grant and Rene has been funded by FCAAP and the NSF I-cubed program. Both Ashley and Rene have been supported by the Undergraduate Research Initiative by the UCF Office of Research and Commercialization.
SURE posters – Ashley, Talia, Rene, David and Spencer
Our laboratory’s strong presence at the Showcase of Undergraduate Research Excellence UCF this year was felt with contributions from Talia and Ashley for their work on metal matrix composites, David and Spencer for their work on Flutter prediction for turbine blades. Rene presented his work from his summer experience at JPL on bulk metallic glass.
Invited Lecture at Harvard University – Dr Raghavan
At the invitation of Professor David Clarke, Dr Raghavan presented a
lecture at the School of Engineering and Applied Sciences, Harvard University. The lecture, “In-situ studies in spectroscopy and synchrotron x-ray diffraction – mapping strain evolution in aerospace materials” was based on the unifying theme of mechanics of materials research conducted in Dr. Raghavan’s laboratory.
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Rene presents at 49th AIAA Aerospace Sciences Meeting, Orlando, FL
Reme Diaz presented his research on “In-Situ Strain Measurements of EB-PVD Thermal Barrier Coatings using Synchrotron X-Ray Diffraction under Thermo-Mechanical Loading.” at the 49th AIAA ASM meeting. The AIAA Aerospace Sciences Meeting is the first major multidisciplinary event of the year for aerospace scientists and engineers from around the world. It provides an ideal forum for scientists and engineers from industry, government, and academia to share and disseminate scientific knowledge and research results with a view toward new technologies for aerospace systems. This meeting is built around excellent technical paper presentation sessions. Rene’s work was funded by FCAAP.